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Diethylene glycol dimethyl ether

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Diethylene glycol dimethyl ether is a colorless, transparent liquid carrying a faint hint of ether scent. Its solubility extends to water, alcohol, and ether, rendering it versatile. Notably, it boasts non-toxic properties while remaining flammable, making it a fascinating compound.

Product Name:

Diethylene glycol dimethyl ether

CAS No.:

111-96-6

Purity

≥99%

Packing:

1ton/drum, 200kg/drum

HScode:

29091990

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Description:

Preparation method:

This compound can be synthesized through the reaction of diethyl alcohol with methanol or by reacting diethylene glycol monomethyl ether with chloromethane (or dimethyl sulfate).
For refining purposes, it is recommended first to treat the compound with granular sodium hydroxide to remove impurities. Subsequently, the purification process involves reflux and vacuum distillation in the presence of calcium hydride, lithium aluminum hydride, sodium borate, or sodium hydride. These operations are conducted in a nitrogen stream to maintain optimal conditions. To address any amine-like odor in diethylene glycol, DME can be effectively eliminated by shaking it with a weakly acidic ion exchange resin before drying and distillation. As an additional precaution, 0.01% sodium boride can be added during storage to prevent peroxide formation.

Synonyms:

1-Methoxy-2-(2-methoxyethoxy)ethane;1,1′-oxybis(2-methoxyethane);2,2′-oxybisethanol dimethyl ether;2,5,8-Trioxanonane;2-Methoxyethyl ether;Diethylene glycol dimethyl ether;diglycol methyl ether;Diglyme;Dimethyl Carbitol;poly solv;methyl diglymer;bis-(2-methoxyethyl)ether;Bis(2-methoxyethyl) Ether;Diethylene Glycol Dimethyl Ether (Diglyme);Diethylene glycol dimethyl ether(DEDM);Diglyme (2-Methoxyethyl Ether);1,1′-Oxybis[2-Methoxy ethane];1-methoxyethoxy-2-methoxyethoxyethane;2,2-OXYBISETHANOLDIBENZOATE;Bis-(2-benzoyloxy-aethyl)-aether;bis-(2-benzoyloxy-ethyl)-ether;Bis(2-methoxyethyl) ether,AcroSeal,Extra Dry;bis(methoxyethyl) ether;DEG dibenzoate;DEGDB;diethyle;diethylenebenzylbenzoate;DIGLYCOL DIBENZOATE;Dimethyldiglycol;DiMe-thyldiglycol;OXY BIS(2-ETHYL BENZOATE);oxydiethylenedibenzoate;Dimethylcarbitol;Bis(2-methoxyethyl) ether;DEDM;glyme2;DIGLYME;Glyme-2;DIYGLME;’DIGLYME’;Poly-Solv;Catafor MS;Dricoid 200;Dariloid 100

Characteristics:

Molecular FormulaC6H14O3
Molar Mass134.17
Density0.944 g/mL at 20 °C (lit.)0.939 g/mL at 25 °C (lit.)
Melting Point-64 °C (lit.)
Boling Point162 °C (lit.)
Flash Point134.6°F
Water SolubilityMiscible
SolubilityMiscible with water and hydrocarbons.
Vapor Presure3 mm Hg ( 20 °C)
Vapor Density4.6 (vs air)
AppearanceColorless liquid
Color≤10(APHA)
OdorMild ethereal.
Maximum wavelength(λmax)[‘λ: 225 nm Amax: 1.00’,
, ‘λ: 240 nm Amax: 0.50’,
, ‘λ: 260 nm Amax: 0.20’,
, ‘λ: 28
Merck143,165
BRN1736101
Storage ConditionStore below +30°C.
StabilityStable. Combustible. Incompatible with strong oxidizing agents. May be air or light sensitive.
SensitiveHygroscopic
Explosive Limit1.4-17.4%(V)
Refractive Indexn20/D 1.408(lit.)
MDLMFCD00008503
PSA:27.7
XLogP3:0.4
Toxicity:LD50 orally in rats: 4.97 g/kg (Smyth)

Use

Diethylene glycol dimethyl ether serves as a non-proton polar solvent, finding application in polar organic reactions, anionic polymerizations, and coordination polymerization reactions as a solvent. It is also used in reduction, alkylation, and condensation reactions. Furthermore, it serves as a medium for Grignard and similar syntheses and acts as an environmentally friendly cleaning agent, extraction solvent, diluent, pharmaceutical adjuvant, and resin solvent.

FAQ:

Q1. What is Diethylene Glycol Dimethyl Ether? 

A1. Diethylene Glycol Dimethyl Ether, commonly known as DGM, is a colorless, odorless, and low-viscosity liquid chemical. It is widely used as a solvent in various industries, including pharmaceuticals, electronics, coatings, and adhesives.

 

Q2. What are the key properties of Diethylene Glycol Dimethyl Ether? 

A2. DGM exhibits excellent solvency power, high boiling point, low vapor pressure, and good stability under normal conditions. It has low viscosity, which makes it suitable for applications requiring rapid evaporation and high heat transfer rates.

 

Q3. What are the main applications of Diethylene Glycol Dimethyl Ether?

A3. DGM finds extensive use as a solvent for polymers, resins, oils, and dyes. It is commonly employed in manufacturing electronics, such as lithium-ion batteries and semiconductors. Additionally, it serves as a valuable component in various laboratory research and industrial processes.

 

Q4. Is Diethylene Glycol Dimethyl Ether safe to handle? 

A4. DGM should be handled with appropriate care. Following good laboratory and industrial practices is important to ensure safe usage. Wearing protective gloves, goggles, and a lab coat while working with DGM is advisable. Please refer to the Safety Data Sheet (SDS) for detailed safety instructions.

 

Q5. What are the storage and handling recommendations for Diethylene Glycol Dimethyl Ether? 

A5. DGM should be stored in a cool, dry, and well-ventilated area away from sources of ignition and direct sunlight. It is advisable to keep containers tightly closed when not in use. Avoid contact with oxidizing agents and incompatible materials. Please refer to the SDS for specific storage and handling guidelines.

 

Q6. How can I order Diethylene Glycol Dimethyl Ether from your company? 

A6. To place an order, please get in touch with our sales team directly through the provided contact information on our website. Our team will be glad to assist you with your requirements, provide product specifications, and offer competitive pricing.

 

Q7. What is the packaging available for Diethylene Glycol Dimethyl Ether?

A7. We offer DGM in various packaging options, including drums, IBC totes, and bulk tanker shipments. The choice of packaging will depend on your specific needs and order quantity. Please consult our sales team to determine the most suitable packaging for your requirements.

 

Q8. Can I get technical support or product customization for Diethylene Glycol Dimethyl Ether? 

A8. Certainly! We provide technical support and can discuss customization options based on your application requirements. Our team of experts will work closely with you to ensure that our product meets your expectations and provides the desired results.

 

Q9. Does your company comply with quality and safety standards for Diethylene Glycol Dimethyl Ether production? 

A9. Yes, we maintain stringent quality control measures and adhere to industry regulations to ensure the production of high-quality and safe DGM. Our manufacturing facilities are equipped with modern technology and operated by trained professionals to guarantee consistent product quality.

 

Q10. Does your company export Diethylene Glycol Dimethyl Ether to other countries? 

A10. Yes, we have experience in exporting Diethylene Glycol Dimethyl Ether to various countries worldwide. Our global distribution network enables us to deliver our products to customers around the globe efficiently. Please get in touch with our sales team to discuss your specific export requirements.

 

Note: The information provided in this FAQ is for general guidance only. For detailed technical specifications, safety information, and specific inquiries, please refer to the product documentation or consult our sales team.

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